TA Instruments

AR1756-0006f

15/03/2013 14:52:24

Sample name	ASW Blank coupon#20 + DI + beads 300rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	6 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:52:24

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	299.9	-509.74	10000	20.0	0.1556	0.996	-166.1	374.9	-0.4432	634.0	242.1740	4.512E-3	302.72	30272	3.411E-3	0.0	0.0
2.0160	299.9	675.84	10000	20.0	0.1209	2.016	220.3	374.9	0.5875	492.7	493.4220	3.505E-3	616.78	61678	3.411E-3	0.0	0.0
3.0120	300.0	665.70	10000	20.0	0.1156	3.012	217.0	375.0	0.5787	471.2	871.7250	3.351E-3	1089.7	1.0897E5	3.411E-3	0.1	0.1
4.0160	300.0	665.76	10000	20.0	0.1120	4.016	217.0	375.0	0.5787	456.3	1121.6600	3.245E-3	1402.1	1.4021E5	3.411E-3	0.1	0.1
5.0120	300.0	654.78	10000	20.0	0.1114	5.012	213.4	375.0	0.5691	453.8	1499.9600	3.227E-3	1875.0	1.8750E5	3.411E-3	0.1	0.1
6.0120	300.0	642.14	10000	20.0	0.1071	6.012	209.3	375.0	0.5581	436.5	1750.1100	3.103E-3	2187.6	2.1876E5	3.411E-3	0.1	0.1
7.0160	300.0	648.99	10000	20.0	0.1152	7.016	211.5	375.0	0.5641	469.5	2001.4200	3.339E-3	2501.8	2.5018E5	3.411E-3	0.1	0.1
8.0000	300.0	652.46	10000	20.0	0.1161	8.000	212.7	375.0	0.5671	472.8	2380.7800	3.363E-3	2976.0	2.9760E5	3.411E-3	0.1	0.1
9.0120	300.0	633.49	10000	20.0	0.1142	9.012	206.5	375.0	0.5507	465.4	2630.2200	3.310E-3	3287.8	3.2878E5	3.411E-3	0.2	0.2
10.012	300.0	639.06	10000	20.0	0.1055	10.012	208.3	375.0	0.5555	429.9	2881.0300	3.057E-3	3601.3	3.6013E5	3.411E-3	0.2	0.2
11.020	300.0	636.77	10000	20.0	0.1148	11.020	207.6	375.0	0.5535	467.9	3258.0400	3.327E-3	4072.6	4.0726E5	3.411E-3	0.2	0.2
12.016	300.0	641.55	10000	20.0	0.1213	12.016	209.1	375.0	0.5576	494.3	3516.0801	3.516E-3	4395.1	4.3951E5	3.411E-3	0.2	0.2
13.012	300.0	633.38	10000	20.0	0.1173	13.012	206.4	375.0	0.5506	477.8	3886.3999	3.398E-3	4858.0	4.8580E5	3.411E-3	0.2	0.2
14.012	300.0	636.79	10000	20.0	0.1075	14.012	207.6	375.0	0.5535	438.1	4139.5498	3.116E-3	5174.4	5.1744E5	3.411E-3	0.2	0.2
15.016	300.0	630.64	10000	20.0	0.1130	15.016	205.6	375.0	0.5481	460.4	4388.9702	3.274E-3	5486.2	5.4862E5	3.411E-3	0.3	0.3
16.016	300.0	639.97	10000	20.0	0.1150	16.016	208.6	375.0	0.5562	468.7	4765.9702	3.333E-3	5957.5	5.9575E5	3.411E-3	0.3	0.3
16.996	300.0	638.91	10000	20.0	0.1092	16.996	208.3	375.0	0.5554	444.7	5017.3701	3.163E-3	6271.7	6.2717E5	3.411E-3	0.3	0.3
18.016	300.0	638.30	10000	20.0	0.1152	18.016	208.1	375.0	0.5548	469.5	5395.6802	3.339E-3	6744.6	6.7446E5	3.411E-3	0.3	0.3
19.020	300.0	645.05	10000	20.0	0.1096	19.020	210.3	375.0	0.5607	446.4	5645.6899	3.175E-3	7057.1	7.0571E5	3.411E-3	0.3	0.3
20.012	300.0	638.74	10000	20.0	0.1132	20.012	208.2	375.0	0.5552	461.3	5896.8901	3.280E-3	7371.1	7.3711E5	3.411E-3	0.3	0.3
21.012	300.0	648.84	10000	20.0	0.1122	21.012	211.5	375.0	0.5640	457.1	6274.0098	3.251E-3	7842.5	7.8425E5	3.411E-3	0.4	0.4
22.016	300.0	633.63	10000	20.0	0.1088	22.016	206.5	375.0	0.5507	443.1	6525.2500	3.151E-3	8156.6	8.1566E5	3.411E-3	0.4	0.4
23.012	300.0	638.75	10000	20.0	0.1169	23.012	208.2	375.0	0.5552	476.2	6905.7700	3.386E-3	8632.2	8.6322E5	3.411E-3	0.4	0.4
24.012	300.0	648.64	10000	20.0	0.1053	24.012	211.4	375.0	0.5638	429.0	7153.4902	3.051E-3	8941.9	8.9419E5	3.411E-3	0.4	0.4
25.016	300.0	645.65	10000	20.0	0.1110	25.016	210.4	375.0	0.5612	452.2	7404.9502	3.215E-3	9256.2	9.2562E5	3.411E-3	0.4	0.4
26.012	300.0	632.80	10000	20.0	0.1077	26.012	206.3	375.0	0.5501	439.0	7781.8599	3.122E-3	9727.3	9.7273E5	3.411E-3	0.4	0.4
27.016	300.0	644.27	10000	20.0	0.1134	27.016	210.0	375.0	0.5600	462.1	8033.4702	3.286E-3	10042	1.0042E6	3.411E-3	0.5	0.5
28.012	300.0	639.39	10000	20.0	0.1191	28.012	208.4	375.0	0.5558	485.2	8284.5000	3.451E-3	10356	1.0356E6	3.411E-3	0.5	0.5
29.012	300.0	631.38	10000	20.0	0.1152	29.012	205.8	375.0	0.5488	469.5	8661.6396	3.339E-3	10827	1.0827E6	3.411E-3	0.5	0.5
30.012	300.0	634.85	10000	20.0	0.1156	30.012	206.9	375.0	0.5518	471.2	8912.8096	3.351E-3	11141	1.1141E6	3.411E-3	0.5	0.5
31.012	300.0	624.96	10000	20.0	0.1191	31.012	203.7	375.0	0.5432	485.2	9289.8799	3.451E-3	11612	1.1612E6	3.411E-3	0.5	0.5
31.996	300.0	631.39	10000	20.0	0.1146	31.996	205.8	375.0	0.5488	467.1	9541.1201	3.321E-3	11926	1.1926E6	3.411E-3	0.5	0.5
33.012	300.0	650.47	10000	20.0	0.1130	33.012	212.0	375.0	0.5654	460.4	9792.6104	3.274E-3	12241	1.2241E6	3.411E-3	0.6	0.6
34.012	300.0	639.23	10000	20.0	0.1242	34.012	208.4	375.0	0.5556	505.9	10169.400	3.598E-3	12712	1.2712E6	3.411E-3	0.6	0.6
35.012	300.0	636.34	10000	20.0	0.1167	35.012	207.4	375.0	0.5531	475.3	10420.800	3.380E-3	13026	1.3026E6	3.411E-3	0.6	0.6
36.016	300.0	642.92	10000	20.0	0.1112	36.016	209.6	375.0	0.5589	453.0	10801.400	3.222E-3	13502	1.3502E6	3.411E-3	0.6	0.6
37.016	300.0	641.13	10000	20.0	0.1136	37.016	209.0	375.0	0.5573	462.9	11049.100	3.292E-3	13811	1.3811E6	3.411E-3	0.6	0.6
38.012	300.0	630.51	10000	20.0	0.1090	38.012	205.5	375.0	0.5480	443.9	11301.700	3.157E-3	14127	1.4127E6	3.411E-3	0.6	0.6
39.012	300.0	638.57	10000	20.0	0.1152	39.012	208.1	375.0	0.5551	469.5	11677.500	3.339E-3	14597	1.4597E6	3.411E-3	0.7	0.7
40.012	300.0	649.19	10000	20.0	0.1116	40.012	211.6	375.0	0.5643	454.7	11928.900	3.233E-3	14911	1.4911E6	3.411E-3	0.7	0.7
41.016	300.0	647.31	10000	20.0	0.1122	41.016	211.0	375.0	0.5627	457.1	12309.300	3.251E-3	15387	1.5387E6	3.411E-3	0.7	0.7
42.016	300.0	637.09	10000	20.0	0.1163	42.016	207.7	375.0	0.5538	473.7	12557.100	3.368E-3	15696	1.5696E6	3.411E-3	0.7	0.7
43.016	300.0	636.09	10000	20.0	0.1130	43.016	207.3	375.0	0.5529	460.4	12809.700	3.274E-3	16012	1.6012E6	3.411E-3	0.7	0.7
44.016	300.0	640.01	10000	20.0	0.1126	44.016	208.6	375.0	0.5563	458.8	13191.400	3.262E-3	16489	1.6489E6	3.411E-3	0.7	0.7
45.012	300.0	634.97	10000	20.0	0.1156	45.012	207.0	375.0	0.5519	471.2	13439.300	3.351E-3	16799	1.6799E6	3.411E-3	0.8	0.8
46.012	300.0	645.60	10000	20.0	0.1069	46.012	210.4	375.0	0.5612	435.6	13689.900	3.098E-3	17112	1.7112E6	3.411E-3	0.8	0.8
47.016	300.0	649.60	10000	20.0	0.1067	47.016	211.7	375.0	0.5647	434.8	14066.300	3.092E-3	17583	1.7583E6	3.411E-3	0.8	0.8
48.012	300.0	637.68	10000	20.0	0.1092	48.012	207.9	375.0	0.5543	444.7	14317.600	3.163E-3	17897	1.7897E6	3.411E-3	0.8	0.8
49.016	300.0	636.71	10000	20.0	0.1122	49.016	207.5	375.0	0.5534	457.1	14694.900	3.251E-3	18369	1.8369E6	3.411E-3	0.8	0.8
50.016	300.0	642.45	10000	20.0	0.1061	50.016	209.4	375.0	0.5584	432.3	14945.700	3.075E-3	18682	1.8682E6	3.411E-3	0.8	0.8
51.012	300.0	625.13	10000	20.0	0.1167	51.012	203.8	375.0	0.5433	475.3	15198.200	3.379E-3	18998	1.8998E6	3.411E-3	0.9	0.9
52.000	300.0	621.64	10000	20.0	0.1205	52.000	202.6	375.0	0.5403	491.0	15576.800	3.491E-3	19471	1.9471E6	3.411E-3	0.9	0.9
53.012	300.0	641.85	10000	20.0	0.1128	53.012	209.2	375.0	0.5579	459.6	15824.500	3.268E-3	19781	1.9781E6	3.411E-3	0.9	0.9
54.016	300.0	641.23	10000	20.0	0.1173	54.016	209.0	375.0	0.5574	477.8	16075.800	3.398E-3	20095	2.0095E6	3.411E-3	0.9	0.9
55.012	300.0	648.04	10000	20.0	0.1108	55.012	211.2	375.0	0.5633	451.4	16452.600	3.210E-3	20566	2.0566E6	3.411E-3	0.9	0.9
56.012	300.0	646.96	10000	20.0	0.1023	56.012	210.9	375.0	0.5623	416.6	16704.900	2.963E-3	20881	2.0881E6	3.411E-3	0.9	0.9
57.016	300.0	637.68	10000	20.0	0.1106	57.016	207.9	375.0	0.5543	450.5	17081.100	3.204E-3	21351	2.1351E6	3.411E-3	1.0	1.0
58.016	300.0	642.22	10000	20.0	0.1130	58.016	209.3	375.0	0.5582	460.4	17332.400	3.274E-3	21666	2.1666E6	3.411E-3	1.0	1.0
59.012	300.0	625.82	10000	20.0	0.1185	59.012	204.0	375.0	0.5440	482.8	17583.600	3.433E-3	21980	2.1980E6	3.411E-3	1.0	1.0
60.012	300.0	634.62	10000	20.0	0.1148	60.012	206.9	375.0	0.5516	467.9	17962.100	3.327E-3	22453	2.2453E6	3.411E-3	1.0	1.0

